['Air Programs']
['Hazardous Air Pollutants']
03/08/2023
...
Table 1 to Subpart QQQQ of Part 63 - Emission Limits for New or Reconstructed Affected Sources
You must comply with the emission limits that apply to your affected source in the following table as required by §63.4690.
If the affected source applies coating to products in the following subcategory. . . | Then, the organic HAP emission limit for the affected source, in grams HAP/liter solids (lb HAP/gal solids) 1 2 is: |
---|---|
1 Determined as a rolling 12-month emission rate according to the requirements in §63.4741, §63.4751, or §63.4761, as applicable. 2 If the affected source applies coatings to products in more than one of the subcategories listed in the table, then you must determine the applicable emission limit according to §63.4690(c). | |
1. Exterior siding and primed doorskins | 0 (0.00) |
2. Flooring | 0 (0.00) |
3. Interior wall paneling or tileboard | 5 (0.04) |
4. Other interior panels | 0 (0.00) |
5. Doors, windows, and miscellaneous | 57 (0.48) |
Table 2 to Subpart QQQQ of Part 63 - Emission Limits for Existing Affected Sources
You must comply with the emission limits that apply to your affected source in the following table as required by §63.4690.
If the affected source applies coating to products in the following subcategory. . . | Then, the organic HAP emission limit for the affected source, in grams HAP/liter solids (lb HAP/gal solids) 1 2 is: |
---|---|
1 Determined as a rolling 12-month emission rate according to the requirements in §63.4741, §63.4751, or §63.4761, as applicable. 2 If the affected source applies coatings to products in more than one of the subcategories listed in the table, then you must determine the applicable emission limit according to §63.4690(c). | |
1. Exterior siding and primed doorskins | 7 (0.06) |
2. Flooring | 93 (0.78) |
3. Interior wall paneling or tileboard | 183 (1.53) |
4. Other interior panels | 20 (0.17) |
5. Doors, windows, and miscellaneous | 231 (1.93) |
Table 3 to Subpart QQQQ of Part 63 - Operating Limits if Using the Emission Rate With Add-On Controls Option
If you are required to comply with operating limits by §63.4692, you must comply with the applicable operating limits in the following table:
For the following device . . . | You must meet the following operating limit . . . | And you must demonstrate continuous compliance with the operating limit by . . . |
---|---|---|
1. Thermal oxidizer | a. The average combustion temperature in any 3-hour period must not fall below the combustion temperature limit established according to §63.4767(a) | i. Collecting the combustion temperature data according to §63.4768(c); ii. Reducing the data to 3-hour block averages; and iii. Maintaining the 3-hour block average combustion temperature at or above the temperature limit. |
2. Catalytic oxidizer | a. The average temperature difference measured across the catalyst bed in any 3-hour period must not fall below the limit established according to §63.4767(b); or | i. Collecting the temperature data according to §63.4768(c); ii. Reducing the data to 3-hour block averages; and iii. Maintaining the 3-hour block temperature difference across the catalyst bed at or above the temperature limit. |
b. Ensure that the inlet temperature of the catalyst bed in any 3-hour period does not fall below the temperature limit established according to §63.4767(b)(2) and develop and implement an inspection and maintenance plan according to §63.4767(b)(3) and (4) | i. Collecting the temperature data according to §63.4768(c), reducing the data to 3-hour block averages, and maintaining the 3-hour average temperature at or above the temperature limit; and ii. Complying with the inspection and maintenance plan developed according to §63.4767(b)(3) and (4). | |
3. Carbon absorber | a. The total regeneration desorbing gas (e.g., steam or nitrogen) mass flow for each carbon bed regeneration cycle must not fall below the total regeneration desorbing gas mass flow limit established according to §63.4767(c) | i. Measuring the total regeneration desorbing gas (e.g., steam or nitrogen) mass flow for each regeneration cycle according to §63.4768(d); and ii. Maintaining the total regeneration desorbing gas mass flow at or above the mass flow limit. |
b. The temperature of the carbon bed, after completing each regeneration and any cooling cycle, must not exceed the carbon bed temperature limit established according to §63.4767(c) | i. Measuring the temperature of the carbon bed, after completing each regeneration and any cooling cycle, according to §63.4768(d); and ii. Operating and carbon beds such that each carbon bed is not returned to service until completing each regeneration and any cooling cycle until the recorded temperature of the carbon bed is at or below the temperature limit. | |
4. Condenser | a. The average condenser outlet (product side) gas temperature in any 3-hour period must not exceed the temperature limit established according to §63.4767(d) | i. Collecting the condenser outlet (product side) gas temperature according to §63.4768(e); ii. Reducing the data to 3-hour block averages; and iii. Maintaining the 3-hour block average gas temperature at the outlet at or below the temperature limit. |
5. Emission capture system that is a PTE according to §63.4765(a) | a. The direction of the air flow at all times must be into the enclosure; and either | i. Collecting the direction of the air flow; and either the facial velocity of air through all natural draft openings according to §63.4768(g)(1) or the pressure drop across the enclosure according to §63.4768(g)(2); and |
ii. Maintaining the facial velocity of air flow through all natural draft openings or the pressure drop at or above the facial velocity limit or pressure drop limit, and maintaining the direction of air flow into the enclosure at all times. | ||
b. The average facial velocity of air through all natural draft openings in the enclosure must be at least 200 feet per minute; or | i. See items 5.a.i and 5.a.ii. | |
c. The pressure drop across the enclosure must be at least 0.007 inch H2O, as established in Method 204 of appendix M to 40 CFR part 51 | i. See items 5.a.i and 5.a.ii. | |
6. Emission capture system that is not a PTE according to §63.4765(a) | a. The average gas volumetric flow rate or duct static pressure in each duct between a capture device and add-on control device inlet in any 3-hour period must not fall below the average volumetric flow rate or duct static pressure limit established for that capture device according to §63.4767(f) | i. Collecting the gas volumetric flow gas or duct static pressure for each capture device according to §63.4768(g); ii. Reducing the data to 3-hour block averages; and iii. Maintaining the 3-hour block average gas volumetric flow rate or duct static pressure for each capture device at or above the gas volumetric flow rate or duct static pressure limit |
7. Concentrators, including zeolite wheels and rotary carbon absorbers | The average gas temperature of the desorption concentrate stream in any 3-hour period must not fall below the limit established according to §63.4767(e); and | i. Collecting the temperature data according to §63.4768(f); ii. Reducing the data to 3-hour block averages; and iii. Maintaining the 3-hour block average temperature at or above the temperature limit. |
b. The average pressure drop of the dilute stream across the concentrator in any 3-hour period must not exceed the limit established according to §63.4767(e) | i. Collecting the pressure drop data according to §63.4768(f); and ii. Reducing the pressure drop data to 3-hour block averages; and iii. Maintaining the 3-hour block average pressure drop at or below at the pressure drop limit. |
Table 4 to Subpart QQQQ of Part 63 - Applicability of General Provisions to Subpart QQQQ of Part 63
You must comply with the applicable General Provisions requirements according to the following table:
Citation | Subject | Applicable to subpart QQQQ | Explanation |
---|---|---|---|
§63.1(a)(1)-(14) | General Applicability | Yes | |
§63.1(b)(1)-(3) | Initial Applicability Determination | Yes | Applicability to subpart QQQQ is also specified in §63.4681. |
§63.1(c)(1) | Applicability After Standard Established | Yes | |
§63.1(c)(2) | Applicability of Permit Program for Area Sources | No | Area sources are not subject to subpart QQQQ. |
§63.1(c)(3) | [Reserved] | No | |
§63.1(c)(4)-(5) | Extensions and Notifications | Yes | |
§63.1(c)(6) | Reclassification | Yes | |
§63.1(d) | [Reserved] | No | |
§63.1(e) | Applicability of Permit Program Before Relevant Standard is Set | Yes | |
§63.2 | Definitions | Yes | Additional definitions are specified in §63.4781. |
§63.3(a)-(c) | Units and Abbreviations | Yes | |
§63.4(a)(1)-(5) | Prohibited Activities | Yes | |
§63.4(b)-(c) | Circumvention/Severability | Yes | |
§63.5(a) | Construction/Reconstruction | Yes | |
§63.5(b)(1)-(6) | Requirements for Existing, Newly Constructed, and Reconstructed Sources | Yes | |
§63.5(c) | [Reserved] | No | |
§63.5(d) | Application for Approval of Construction/Reconstruction | Yes | |
§63.5(e) | Approval of Construction/Reconstruction | Yes | |
§63.5(f) | Approval of Construction/Reconstruction Based on Prior State Review | Yes | |
§63.6(a) | Compliance With Standards and Maintenance Requirements - Applicability | Yes | |
§63.6(b)(1)-(7) | Compliance Dates for New and Reconstructed Sources | Yes | §63.4683 specifies compliance dates. |
§63.6(c)(1)-(5) | Compliance Dates for Existing Sources | Yes | §63.4683 specifies compliance dates. |
§63.6(d) | [Reserved] | No | |
§63.6(e)(1)(i) | General Duty to Minimize Emissions | No | See §63.4700(b) for general duty requirement. |
§63.6(e)(1)(ii) | Requirement to Correct Malfunctions ASAP | No | |
§63.6(e)(1)(iii) | Operation and Maintenance Requirements Enforceable Independent of Emissions Limitations | Yes | |
§63.6(e)(2) | [Reserved] | No | |
§63.6(e)(3) | SSMP | No | |
§63.6(f)(1) | Compliance Except During SSM | No | |
§63.6(f)(2)-(3) | Methods for Determining Compliance | Yes | |
§63.6(g)(1)-(3) | Use of an Alternative Standard | Yes | |
§63.6(h) | Compliance with Opacity/Visible Emissions Standards | No | Subpart QQQQ does not establish opacity standards and does not require continuous opacity monitoring systems (COMS). |
§63.6(i)(1)-(16) | Extension of Compliance | Yes | |
§63.6(j) | Presidential Compliance Exemption | Yes | |
§63.7(a)(1) | Performance Test Requirements - Applicability | Yes | Applies to all affected sources. Additional requirements for performance testing are specified in §§63.4751, 63.4752, 63.4764, 63.4765, and 63.4766. |
§63.7(a)(2) | Performance Test Requirements - Dates | Yes | Applies only to performance tests for capture system and control device efficiency at sources using these to comply with the standard. §63.4760 specifies the schedule for performance test requirements that are earlier than those specified in §63.7(a)(2). |
§63.7(a)(3) | Performance Tests Required By the Administrator | Yes | |
§63.7(a)(4) | Notification of Delay in Performance Testing Due to Force Majeure | Yes | |
§63.7(b)-(d) | Performance Test Requirements - Notification, Quality Assurance, Facilities Necessary for Safe Testing, Conditions During Test | Yes | Applies only to performance tests for capture system and add-on control device efficiency at sources using these to comply with the standard. |
§63.7(e)(1) | Performance Testing | Yes | |
§63.7(f) | Performance Test Requirements - Use of Alternative Test Method | Yes | Applies to all test methods except those used to determine capture system efficiency. |
§63.7(g)-(h) | Performance Test Requirements - Data Analysis, Recordkeeping, Reporting, Waiver of Test | Yes | Applies only to performance tests for capture system and add-on control device efficiency at sources using these to comply with the standard. |
§63.8(a)(1)-(2) | Monitoring Requirements - Applicability | Yes | Applies only to monitoring of capture system and add-on control device efficiency at sources using these to comply with the standard. Additional requirements for monitoring are specified in §63.4768. |
§63.8(a)(3) | [Reserved] | No | |
§63.8(a)(4) | Additional Monitoring Requirements | No | Subpart QQQQ does not have monitoring requirements for flares. |
§63.8(b) | Conduct of Monitoring | Yes | |
§63.8(c)(1) | Continuous Monitoring System (CMS) Operation and Maintenance | Yes | Applies only to monitoring of capture system and add-on control device efficiency at sources using these to comply with the standard. Additional requirements for CMS operations and maintenance are specified in §63.4768. |
§63.8(c)(1)(i) | General Duty to Minimize Emissions and CMS Operation | No | |
§63.8(c)(1)(ii) | Operation and Maintenance of CMS | Yes | |
§63.8(c)(1)(iii) | Requirement to Develop SSM Plan for CMS | No | |
§63.8(c)(2)-(3) | Monitoring System Installation | Yes | |
§63.8(c)(4) | CMSs | No | §63.4768 specifies the requirements for the operation of CMS for capture systems and add-on control devices at sources using these to comply. |
§63.8(c)(5) | COMS | No | Subpart QQQQ does not have opacity for visible emission standards. |
§63.8(c)(6) | CMS Requirements | Yes | §63.4768 specifies the requirements for monitoring systems for capture systems and add-on control devices at sources using these to comply. |
§63.8(c)(7) | CMS Out-of-Control Periods | Yes | |
§63.8(c)(8) | CMS Out-of-Control Periods Reporting | No | §63.4720 requires reporting of CMS out-of-control periods. |
§63.8(d)-(e) | Quality Control Program and CMS Performance Evaluation | No | Subpart QQQQ does not require the use of continuous emissions monitoring systems. |
§63.8(f)(1)-(5) | Use of an Alternative Monitoring Method | Yes | |
§63.8(f)(6) | Alternative to Relative Accuracy Test | No | Subpart QQQQ does not require the use of continuous emissions monitoring systems. |
§63.8(g)(1)-(5) | Data Reduction | No | §§63.4767 and 63.4768 specify monitoring data reduction. |
§63.9(a)-(d) | Notification Requirements | Yes | |
§63.9(e) | Notification of Performance Test | Yes | Applies only to capture system and add-on control device performance tests at sources using these to comply with the standard. |
§63.9(f) | Notification of Visible Emissions/Opacity Test | No | Subpart QQQQ does not have opacity or visible emission standards. |
§63.9(g)(1)-(3) | Additional Notifications When Using CMS | No | Subpart QQQQ does not require the use of continuous emissions monitoring systems. |
§63.9(h) | Notification of Compliance Status | Yes | §63.4710 specifies the dates for submitting the Notification of Compliance Status. |
§63.9(i) | Adjustment of Submittal Deadlines | Yes | |
§63.9(j) | Change in Previous Information | Yes | |
§63.9(k) | Electronic reporting procedures | Yes | Only as specified in §63.9(j). |
§63.10(a) | Recordkeeping/Reporting - Applicability and General Information | Yes | |
§63.10(b)(1) | General Recordkeeping Requirements | Yes | Additional requirements are specified in §§63.4730 and 63.4731. |
§63.10(b)(2)(i)-(ii) | Recordkeeping of Occurrence and Duration of Startups and Shutdowns | No | |
§63.10(b)(2)(iii) | Recordkeeping Relevant to CMS | Yes | |
§63.10(b)(2)(iv)-(v) | Recordkeeping Relevant to SSM | No | |
§63.10(b)(2)(vi)-(xi) | Recordkeeping for CMS Malfunctions | Yes | |
§63.10(b)(2)(xii) | Records | Yes | |
§63.10(b)(2)(xiii) | No | Subpart QQQQ does not require the use of continuous emissions monitoring systems. | |
§63.10(b)(2)(xiv) | Yes | ||
§63.10(b)(3) | Recordkeeping Requirements for Applicability Determinations | Yes | |
§63.10(c)(1)-(6) | Additional Recordkeeping Requirements for Sources with CMS | Yes | |
§63.10(c)(7)-(8) | No | The same records are required in §63.4720(a)(7). | |
§63.10(c)(9)-(14) | Yes | ||
§63.10(c)(15) | Use of SSM Plan | No | |
§63.10(d)(1) | General Reporting Requirements | Yes | Additional requirements are specified in §63.4720. |
§63.10(d)(2) | Report of Performance Test Results | Yes | Additional requirements are specified in §63.4720(b). |
§63.10(d)(3) | Reporting Opacity or Visible Emissions Observations | No | Subpart QQQQ does not require opacity or visible emissions observations. |
§63.10(d)(4) | Progress Reports for Sources With Compliance Extensions | Yes | |
§63.10(d)(5) | SSM Reports | No | Malfunctions shall be reported based on compliance option under §63.4720(a)(5-7). |
§63.10(e)(1)-(2) | Additional CMS Reports | No | Subpart QQQQ does not require the use of continuous emissions monitoring systems. |
§63.10(e)(3) | Excess Emissions/CMS Performance Reports | No | §63.4720(b) specifies the contents of periodic compliance reports. |
§63.10(e)(4) | COMS Data Reports | No | Subpart QQQQ does not specify requirements for opacity or COMS. |
§63.10(f) | Recordkeeping/Reporting Waiver | Yes | |
§63.11 | Control Device Requirements/Flares | No | Subpart QQQQ does not specify use of flares for compliance. |
§63.12 | State Authority and Delegations | Yes | |
§63.13 | Addresses | Yes | |
§63.14 | Incorporation by Reference | Yes | Test Methods ANSI A135.4-2012, ANSI/ASME PTC 19.10-1981, Part 10, ASTM D1475-13, ASTM D2111-10 (Reapproved 2015), ASTM D2369-10 (Reapproved 2015) e, ASTM D2697-03 (Reapproved 2014), ASTM D4840-99 (2018) e, ASTM D6093-97 (Reapproved 2016), ASTM D6348-03 (Reapproved 2010) and NCASI Method ISS/FP A105.01 (incorporated by reference, see §63.14). |
§63.15 | Availability of Information/Confidentiality | Yes | |
§63.16 | Requirements for Performance Track Member Facilities | Yes |
[84 FR 7705, Mar. 4, 2019; 85 FR 73908, Nov. 19, 2020]
Table 5 to Subpart QQQQ of Part 63 - Default Organic HAP Mass Fraction for Solvents and Solvent Blends
You may use the mass fraction values in the following table for solvent blends for which you do not have test data or manufacturer's formulation data.
Solvent/solvent blend | CAS. No. | Average organic HAP mass fraction | Typical organic HAP, percent by mass |
---|---|---|---|
1. Toluene | 108-88-3 | 1.0 | Toluene. |
2. Xylene(s) | 1330-20-7 | 1.0 | Xylenes, ethylbenzene. |
3. Hexane | 110-54-3 | 0.5 | n-hexane. |
4. n-Hexane | 110-54-3 | 1.0 | n-hexane. |
5. Ethylbenzene | 100-41-4 | 1.0 | Ethylbenzene. |
6. Aliphatic 140 | 0 | None. | |
7. Aromatic 100 | 0.02 | 1% xylene, 1% cumene. | |
8. Aromatic 150 | 0.09 | Naphthalene. | |
9. Aromatic naphtha | 64742-95-6 | 0.02 | 1% xylene, 1% cumene. |
10. Aromatic solvent | 64742-94-5 | 0.1 | Naphthalene. |
11. Exempt mineral spirits | 8032-32-4 | 0 | None. |
12. Ligroines (VM & P) | 8032-32-4 | 0 | None. |
13. Lactol spirits | 64742-89-6 | 0.15 | Toluene. |
14. Low aromatic white spirit | 64742-82-1 | 0 | None. |
15. Mineral spirits | 64742-88-7 | 0.01 | Xylenes. |
16. Hydrotreated naphtha | 64742-48-9 | 0 | None. |
17. Hydrotreated light distillate | 64742-47-8 | 0.001 | Toluene. |
18. Stoddard solvent | 8052-41-3 | 0.01 | Xylenes. |
19. Super high-flash naphtha | 64742-95-6 | 0.05 | Xylenes. |
20. Varsol ® solvent | 8052-49-3 | 0.01 | 0.5% xylenes, 0.5% ethylbenzene. |
21. VM & P naphtha | 64742-89-8 | 0.06 | 3% toluene, 3% xylene. |
22. Petroleum distillate mixture | 68477-31-6 | 0.08 | 4% naphthalene, 4% biphenyl. |
Table 6 to Subpart QQQQ of Part 63 - Default Organic HAP Mass Fraction for Petroleum Solvent Groups a
You may use the mass fraction values in the following table for solvent blends for which you do not have test data or manufacturer's formulation data.
Solvent type | Average organic HAP mass fraction | Typical organic HAP, percent by mass |
---|---|---|
a Use this table only if the solvent blend does not match any of the solvent blends in Table 5 to this subpart and you only know whether the blend is aliphatic or aromatic. bE.g., Mineral Spirits 135, Mineral Spirits 150 EC, Naphtha, Mixed Hydrocarbon, Aliphatic Hydrocarbon, Aliphatic Naphtha, Naphthol Spirits, Petroleum Spirits, Petroleum Oil, Petroleum Naphtha, Solvent Naphtha, Solvent Blend. cE.g., Medium-flash Naphtha, High-flash Naphtha, Aromatic Naphtha, Light Aromatic Naphtha, Light Aromatic Hydrocarbons, Aromatic Hydrocarbons, Light Aromatic Solvent. | ||
Aliphatic b | 0.03 | 1% xylene, 1% toluene, and 1% ethylbenzene. |
Aromatic c | 0.06 | 4% xylene, 1% toluene, and 1% ethylbenzene. |
Table 7 to Subpart QQQQ of Part 63—List of HAP That Must Be Counted Toward Organic HAP Content if Present at 0.1 Percent or More by Mass
Chemical name | CAS No. |
---|---|
1,1,2,2-Tetrachloroethane | 79-34-5 |
1,1,2-Trichloroethane | 79-00-5 |
1,1-Dimethylhydrazine | 57-14-7 |
1,2-Dibromo-3-chloropropane | 96-12-8 |
1,2-Diphenylhydrazine | 122-66-7 |
1,3-Butadiene | 106-99-0 |
1,3-Dichloropropene | 542-75-6 |
1,4-Dioxane 123-91-1 | |
2,4,6-Trichlorophenol | 88-06-2 |
2,4/2,6-Dinitrotoluene (mixture) | 25321-14-6 |
2,4-Dinitrotoluene | 121-14-2 |
2,4-Toluene diamine | 95-80-7 |
2-Nitropropane | 79-46-9 |
3,3?-Dichlorobenzidine | 91-94-1 |
3,3?-Dimethoxybenzidine | 119-90-4 |
3,3?-Dimethylbenzidine | 119-93-7 |
4,4?-Methylene bis(2-chloroaniline) | 101-14-4 |
Acetaldehyde | 75-07-0 |
Acrylamide | 79-06-1 |
Acrylonitrile | 107-13-1 |
Allyl chloride | 107-05-1 |
alpha-Hexachlorocyclohexane (a-HCH) | 319-84-6 |
Aniline | 62-53-3 |
Benzene | 71-43-2 |
Benzidine | 92-87-5 |
Benzotrichloride | 98-07-7 |
Benzyl chloride | 100-44-7 |
beta-Hexachlorocyclohexane (b-HCH) | 319-85-7 |
Bis(2-ethylhexyl)phthalate | 117-81-7 |
Bis(chloromethyl)ether | 542-88-1 |
Bromoform | 75-25-2 |
Captan | 133-06-2 |
Carbon tetrachloride | 56-23-5 |
Chlordane | 57-74-9 |
Chlorobenzilate | 510-15-6 |
Chloroform | 67-66-3 |
Chloroprene | 126-99-8 |
Cresols (mixed) | 1319-77-3 |
DDE | 3547-04-4 |
Dichloroethyl ether | 111-44-4 |
Dichlorvos | 62-73-7 |
Epichlorohydrin | 106-89-8 |
Ethyl acrylate | 140-88-5 |
Ethylene dibromide | 106-93-4 |
Ethylene dichloride | 107-06-2 |
Ethylene oxide | 75-21-8 |
Ethylene thiourea | 96-45-7 |
Ethylidene dichloride (1,1-Dichloroethane) | 75-34-3 |
Formaldehyde | 50-00-0 |
Heptachlor | 76-44-8 |
Hexachlorobenzene | 118-74-1 |
Hexachlorobutadiene | 87-68-3 |
Hexachloroethane | 67-72-1 |
Hydrazine | 302-01-2 |
Isophorone | 78-59-1 |
Lindane (hexachlorocyclohexane, all isomers) | 58-89-9 |
m-Cresol | 108-39-4 |
Methylene chloride | 75-09-2 |
Naphthalene | 91-20-3 |
Nitrobenzene | 98-95-3 |
Nitrosodimethylamine | 62-75-9 |
o-Cresol | 95-48-7 |
o-Toluidine | 95-53-4 |
Parathion | 56-38-2 |
p-Cresol | 106-44-5 |
p-Dichlorobenzene | 106-46-7 |
Pentachloronitrobenzene | 82-68-8 |
Pentachlorophenol | 87-86-5 |
Propoxur | 114-26-1 |
Propylene dichloride | 78-87-5 |
Propylene oxide | 75-56-9 |
Quinoline | 91-22-5 |
Tetrachloroethene | 127-18-4 |
Toxaphene | 8001-35-2 |
Trichloroethylene | 79-01-6 |
Trifluralin | 1582-09-8 |
Vinyl bromide | 593-60-2 |
Vinyl chloride | 75-01-4 |
Vinylidene chloride | 75-35-4 |
Source: 68 FR 31760, May 28, 2003, unless otherwise noted.
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